47 g), in a 1000 mL three-neck round bottom flask with the initiator AIBN
The copolymerization of NPAM monomer with MMA was carried using AIBN
as a free radical initiator in THF at 65[degrees]C (described below and shown in Scheme 3).
Azobis-isobutyronitrile ANN Artificial Neural Network b correlation parameter c correlation parameter [C.
2) with an initiator loading of 50 mM AIBN
and for an initial mole fraction of styrene ([f.
The kinetic scheme of free radical bulk copolymerization of styrene and acrylonitrile, using AIBN
as the initiator, is summarized in Table 1.
Then calculated quantities of ATBS and initiator AIBN
The AFM height image in Figure 7 was taken on the same material as the SEM image in Figure 6C (MMA/alkyd with AIBN
as the initiator).
Ten-millilitre MMA or DMAAm, 10 mL DMSO, and AIBN
were added into a three-necked round-bottom flask with a magnetic stirring bar.
A mixture of NIPAAm, PEGDAc, PCLDAc, AIBN
, and 1,4-dioxane was put into a glass tube, degassed three times by freeze-thaw-pump cycles, and sealed under argon.
and a predetermined amount of MMSA was transferred into each Schlenk tube.
Free radical homopolymerization and copolymerization reactions of St and FSt were carried out in the bulk using AIBN
as the initiator.
, and acetonitrile are further purified by distillation, whereas the other chemicals are used as received without further purification.