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BSTFA |
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Therefore, the material was derivatized with BSTFA and analyzed by GC-MS. After drying under a stream of argon, the samples were dissolved in 100 [micro]L methylene chloride and derivatized with BSTFA following the manufacturer's instructions. Seven calibration standards, ranging from 15 to 1,000 ng/[micro]L, were prepared in acetonitrile and derivatized using BSTFA under the same conditions as samples before GC-MS analysis. |
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