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2] and is maintained above 80 [degrees] C for at least two hours to remove the chlorotrimethylsilane by-product by The inherent viscosity of the polyimide synthesized was double in the presence of chlorotrimethylsilane (TMSCI) compared with that of the polyimide made without the activator. 2]CuLi) containing chlorotrimethylsilane (16) at low temperature cleanly afforded the desired 1,6-addition products in high yields (Table 1). |
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