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GC-ECD |
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The aliquot of oil was first placed on aminopropyl solid phase extraction (SPE) columns, eluted with hexane, concentrated, and analyzed by GC-ECD equipped with a capillary column coated with a nonpolar stationary phase [5 % (mole fraction) phenyl methylpolysiloxane, DB-5, J & W Scientific, Folsom, CA]. Determination of PCBs and organochlorine pesticides by GC-ECD and GC/MS. Liquid chromatography was used for the isolation of the Aroclors from the transformer oil SRMs prior to GC-ECD analysis. |
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