GC-MSDGas Chromatography and Mass Selective Detection
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Louis, USA) as stationary phase and methanol (Merck Millipore, Darmstadt, Germany) as eluent, which was concentrated and analyzed by GC-MSD.
Metabolite identification: We analyzed the unconcentrate organic phase using GC-FID; it showed 12 volatile metabolites, which we identified using GC-MSD analysis.
Part 1 - Chromatography GC-MSD assembly with the liquid feed;