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HNO3 |
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The plasma conditions were kept constant during analysis of standards, instrument blanks and laser-ablated samples by constantly aspirating a 1% HNO3 solution, which was the matrix for both the standards and the blanks (see Zacherl et al. For the determination of total element concentrations (Cd, Cu, Pb, Cr, Zn, As, V, Ba, and Hg) in the cyclone ash, the dried sample was decomposed (digested) with a mixture of HCl (3 mL) and HNO3 (9 mL) in a CEM Mars 5 microprocessor controlled microwave oven with CEM HP 500 Teflon vessels (CEM corp. For that reason we did not use HNO3 to decrease the content of pyritic sulphur. |
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