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CIDNPChemically Induced Dynamic Nuclear Polarization
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The initial radical reaction steps of the photodecomposition was recently studied by CIDNP (14) and laser spectroscopy (11).
CIDNP experiments lead to the conclusion that hydrogen abstraction occurs in the primary radical pair, leading to methyl thio benzaldehyde.
Robinson, FCIC Mechanistic studies being undertaken by Robinson include synthesis and thermolysis of optically active and isotopically labeled azo compounds, using kinetic methods and CIDNP. Studies have involved structure-reactivity correlations on pyridine and naphthlene derivations, by pKa measurements and 1H and 19F nuclear magnetic resonance spectroscopy.