CPTMSCanadian Penning Trap Mass Spectrometer
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In the present work, amine functionalized silica catalysts, including NH2/SiO2, DBU/SiO2 and TBD/SiO2, were prepared with APTMS and 3- chloropropyltrimethoxysilane (CPTMS) as the coupling agents by ultrasonic technique under mild experimental conditions.
TBD/SiO2 was prepared by two steps: silica was firstly modified by CPTMS via the same method as that of NH2/SiO2, and chloropropylsilyl- functionalized SiO2 was then reacted with 0.05 mol TBD in cyclohexane (40.0 mL).