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References in periodicals archive ?
Keywords: Tolterodine, dansyl chloride, pharmaceutical preparations, plasma, derivatization
Development of a rapid and sensitive LC-ESI/MS/MS assay for the quantification of propofol using a simple off-line dansyl chloride derivatization reaction to enhance signal intensity J Pharm Biomed Anal 2005; 39: 411-7.
LC-ESI(+)-MS/MS was reported for analysis of 14 OH-PBDEs in serum following derivatisation with dansyl chloride.
Derivatization with dansyl chloride, as described below, was highly effective and was therefore used for all studies described for the LC-MS/MS method (31).
To derivatize the samples, we then added an equal volume of 1 g/L dansyl chloride in acetone, vortex-mixed each sample for 1 min, and incubated the samples in a heating block at 60[degrees]C for 3 min.
Samples were derivatized with dansyl and separated on a C18 column with a solvent gradient system between two buffers containing 125 mL/L and 500 mL/L acetonitrile.
The urinary 3-methylhistidine concentrations were determined by reversed-phase HPLC after precolumn derivatization with dansyl chloride (15) and fluorescence detection.
The use of reverse-phase high-performance liquid chromatography and precolumn derivatization with dansyl chloride for quantitation of specific amino acids in collagen and elastin.
Synthesis and use of labelled nucleoside phosphoramidite building blocks bearing a reporter group: biotinyl, dinitrophenyl, pyrenyl and dansyl.
Evaluation of samplecollection, storage and derivatization conditions for analysis of dansyl derivatives by HPLC.
37) described the application of environmentally sensitive dansyl probe, connected to the [beta]-cyclodextrin and trapped in a porous sol-gel glass matrix for bomeol detection.
Gal-Hyl can be measured using an amino acid analyzer (12), but simpler methods have been developed for measurement of urinary Gal-Hyl, using HPLC after derivatization with dansyl chloride (13-16).