GC-FPDGas Chromatography with Flame Photometric Detection
GC-FPDGas Chromatography with Flame Photometric Detector
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[25] Linearity range (ppm) 0.5-100 5-100 Linearity regression 0.998 0.997 Sensitivity (ppm) 0.1 2 RSD (%, 10-15 ppm)/intra-day 1.4 (n = 8) 3.0 RSD (%, 10-15 ppm)/inter-day 4.3 (n = 4) 5.1 Sample preparation needed SPE procedure No Detection Exxon and Skydrol Skydrol GC-FPD method Spila et al.
The concentrated derivatives were dissolved in ethyl acetate (2.0 mL) and filtered through a 0.22 [micro]m polytetrafluoroethylene (PTFE) membrane filter prior to analysis by GC-FPD.
Simple determination of 40 organophosphate pesticides in raw wool using microwave-assisted extraction and GC-FPD analysis.
The contents were then mixed in a vortex mixer for 3 sec prior to injection into the GC-FPD. The same procedure was adopted for both the untreated and treated from the field trial samples before injection into the GC-FPD, with the exception of the spiked standard solutions.