HPDSCHigh Pressure Differential Scanning Calorimetry
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The HPDSC measurements were performed at 5 MPa pressure in nitrogen atmosphere in a DSC (Mettler TA 8000 with DSC27HP pressure cell) in the temperature range 30 [degrees] C to 225 [degrees] C at a heating rate of 5 [degrees] C/min.
The results from a HPDSC measurement of a nonheated TSA sample are presented in Fig.
Nevertheless, the HPDSC measurements of the fractional conversions at the second tan[Delta] maxima do not give a clear answer whether the maxima correspond to gelation or not.
Such a measurement is, however, not useful in this case, since [T.sub.g] cannot be observed, at least not with the available HPDSC equipment.