LC-EDLiquid Chromatography with Electrochemical Detector
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Identity and purity of the DOPAL standard was tested by mass spectroscopy and nuclear magnetic resonance (NMR) at the time of synthesis and confirmed by liquid chromatography with electrochemical detection (LC-ED) and LC-TOF-MS as part of the present study.
Droxidopa injected directly into the LC-ED system contained DOPAL (Fig.
[3] Nonstandard abbreviations: L-DOPS, L-threo-3,4-dihydroxyphenylserine; NE, norepinephrine; DOPAL, dihydroxyphenylacetaldehyde; PAD, pure autonomic failure; MSA, multiple system atrophy; DOPA, dihydroxyphenylalanine; NMR, nuclear magnetic resonance; LC-ED, liquid chromatography with electrochemical detection; IV, intravenous.