TG-DTAThermogravimetric/Differential Thermal Analyzer
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Also characterised of sample determine by XRD, FTIR, I-V, TG-DTA, EDS, SEM, chemical and thermal analyses were used to investigate the structure, morphology, and composition of the obtained product.
TG-DTA. From TG-DTA graph (Figure 1(d)) initially due to the removal of the surface deposited moisture or solvent molecules on the powder, a little weight loss was observed in between 0 and 110[degrees]C.
PXRD measurement and TG-DTA measurement suggested inclusion complex formation in FD (MT/[alpha]CD) and FD (MT/[gamma]CD).
TG-DTA results showed the thermal stability of HAP powder obtained from hen's egg-shell.
Moreover, the thermogravimetric analysis and differential thermal analysis (TG-DTA) curves of the samples were carried out by CRY-2P and WRT-3P analyzer.
The TG-DTA curves of resultant 2 in air from room temperature to 1023 K are shown in Figure 1.
Based on XRD and TG-DTA results as well as considering the above factors, the calcination of the intermediate layer was carried out at 450[degrees]C for 1 h.
The volume of crushed coal particles was less than that of the platinum container placed in TG-DTA which is almost equal to 49.1 [mm.sup.3] as shown in Figure 2.
The [O.sub.2] content and excess air ratio was higher and was responsible for high CO and NOx emission, ii) The TG-DTA analysis suggested that the combustion of the sludge separated from swine wastewater treatment plants could be processed in three stages.