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The prepared ThGA decorated Mn NP was added to the above solution.
Various analytical techniques were employed to analyze the synthesized ThGA decorated Mn NP end capped PCL.
Figure 1 a displays the FTIR spectrum of ThGA decorated Mn NP.
The TEM image of ThGA decorated Mn NP end capped PCL is shown in Fig.
The yellow region in the micrograph is the PCL matrix and the presence of sharp white peaks is due to the incorporated ThGA decorated metal salt.
The main purpose of this measurement is to know the crystallization behavior of the prepared ThGA decorated Mn NP end capped PCL under non-isothermal condition.
The obtained [E.sub.a] value is higher when compared with pure PCL (142 kJ [mol.sup.-1]) , This is due to the incorporation of nano-sized ThGA decorated Mn into PCL chain.
The thermal stability of ThGA decorated Mn NP end capped PCL was inspected using TGA technique.
The thermal degradation of ThGA decorated Mn NP end capped PCL was analyzed using TGA measurements at five different heating rates such as 10, 15, 20, 25, and 30[degrees]C [min.sup.-1] under air atmosphere.
The analysis of the various SRM materials clearly demonstrates the ability of the PinAAcle 900T spectrometer to generate quality data incorporating THGA tubes, longitudinal Zeeman background correction and STPF conditions for interference-free, accurate quantitation.
* In the analysis of SRM materials, PerkinElmer's spectrometer generated quality data incorporating THGA tubes, longitudinal Zeeman background correction and STPF conditions.
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