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References in periodicals archive ?
In the studies of the WAXD analysis, it was observed that the affinity between the ABS and clay which contained benzyl group was better than that of the PP and clay.
2 shows, the degree of substitution of benzyl groups was proportional to the degree of sodium-metallation of PMIA(Na/CONH).
The number average molecular weight (Mn) of the benzylated PMIA measured by GPC, however, decreased with an increasing degree of substitution of benzyl groups. This may be caused by either the scission of amide bonds or the change of the shape of PMIA molecules owing to the sodium-metallation and the alkylation reactions.
As expected, intensity of the signals, above described, increases when the BzOH/ Ti[Cl.sub.4] ratio decreases, consolidating the XRD and gravimetric analysis data that show, in the case of T_S50, the presence of unknown phase (probably due to the uncondensed benzyl groups) and the highest mass loss, respectively.
The benzyl groups of 6 were removed by boron tribromide in dichloromethane and replaced with mesyl groups resulting in compound 8.
Keeping in view the biological properties of octahydroquinazolines [1-3], we have recently reported [4, 5] the synthesis of hexahydroquinazolin-5(6H)-ones bearing phenyl and benzyl groups in position 1 of the ring and bis-hexahydroquinazolin-5(6H)-ones bearing phenyl group in position 1 of the ring.
The peak intensity ratio of the phenyl to the benzyl groups was 5.29/2.00, higher than the calculated values (4/2) assuming that the benzyl chloride moiety was kept intact [33].